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KMID : 0525720200250020072
Journal of Chitin and Chitosan
2020 Volume.25 No. 2 p.72 ~ p.77
Preparation of Alpha-Chitosan Nanofiber Aqueous Solution via Aqueous Counter Collision Treatment
Kim Joong-Kwon

Jin Jung-Ho
Seo Won-Jeong
Yun Yu-Jeong
Jeon Hyeon-Kyu
Abstract
The aim of this study is to investigate the effect of ¥á-chitosan nanofibrillation on the efficacy of preparing aqueous chitosan solution. The solution process of ¥á-chitosan is essential to afford chitosan-based functional materials in various forms, such films, fibers, sponges, and hydrogels. In terms of solution process, the nanofibrillation of ¥á-chitosan is generally reported as an efficient way of preparing homogeneous aqueous solutions since it allows an improved solubility of ¥á-chitosan in acidic aqueous media. In this article, we perform a nanofibrillation of ¥á-chitosan to obtain chitosan nanofibers using an aqueous counter collision (ACC) treatment technique. We investigate the morphology, crystallinity, and chemical structure of the ACC-derived ¥á-chitosan nanofibers using SEM, XRD, and FT-IR. Consequently, we show that the ACC-assisted nanofibrillation of ¥á-chitosan can afford a rapid preparation of homogeneous aqueous solution of ¥á-chitosan powder in typical acidic water.
KEYWORD
Chitosan, Aqueous counter collision, Acetic acid, Lactic acid, Dissolution
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